C₃₈H₅₂N₅O₄

Base Information

• Chemical Name: C₃₈H₅₂N₅O₄
• CAS No.: 1236153-29-9
• Molecular Formula: C₃₈H₅₂N₅O₄
• Molecular Weight: 642.862
• Mol file: 1236153-29-9.mol

Synonyms:C₃₈H₅₂N₅O₄

Chemical Property of C₃₈H₅₂N₅O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₅₂N₅O₄

There total 11 articles about C₃₈H₅₂N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C40H54N5O5 → C38H52N5O4 (1236153-29-9)

Guidance literature:

With sodium hydroxide; In methanol; for 2h; Inert atmosphere;

DOI:10.1016/j.bmcl.2011.12.091

Reference yield:

C40H52N5O5 (1236153-28-8) → C38H52N5O4 (1236153-29-9)

Guidance literature:

With methanol; sodium hydroxide; for 2h;

Reference yield:

11β-[4-(2-tosyloxyethoxy)-phenyl]-estra-4,9-diene-3,17-dione (1236153-19-7) → C38H52N5O4 (1236153-29-9)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium azide / ethanol / 4 h / 81 °C / Inert atmosphere

2: Acetyl bromide / dichloromethane / 4 h / Inert atmosphere

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 60 °C / Inert atmosphere

4: sodium tetrahydroborate / methanol / 2 h / Inert atmosphere

5: sodium hydroxide / methanol / 2 h / Inert atmosphere

With sodium tetrahydroborate; sodium azide; copper(ll) sulfate pentahydrate; Acetyl bromide; sodium L-ascorbate; sodium hydroxide; In methanol; ethanol; dichloromethane; water; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2011.12.091

upstream raw materials:

C₄₀H₅₂N₅O₅

2,2,6,6-tetramethyl-4-(prop-2-ynylamino)-piperidone nitroxide

11β-[4-(2-tosyloxyethoxy)-phenyl]-estra-4,9-diene-3,17-dione

11β-[4-(2-azidoethoxy)phenyl]estra-4,9-diene-3,17-dione