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Technology Process of 3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide

3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide

Base Information
  • Chemical Name:3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide
  • CAS No.:666746-35-6
  • Molecular Formula:C21H20F3IN2O2
  • Molecular Weight:516.302
  • Hs Code.:
3-iodo-N<sub>2</sub>-isopropyl-N<sub>1</sub>-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide

Synonyms:3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide

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Chemical Property of 3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide
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Technology Process of 3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide

There total 1 articles about 3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-4-(1-trifluoromethylethenyl)aniline
666746-34-5

2-methyl-4-(1-trifluoromethylethenyl)aniline

3-iodo-N-isopropylphthalamidic acid
226979-91-5

3-iodo-N-isopropylphthalamidic acid

3-iodo-N<sub>2</sub>-isopropyl-N<sub>1</sub>-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide
666746-35-6

3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide

Guidance literature:
3-iodo-N-isopropylphthalamidic acid; With trifluoroacetic anhydride; In toluene; at 20 ℃; for 0.5h;
2-methyl-4-(1-trifluoromethylethenyl)aniline; In tetrahydrofuran; at 20 ℃; for 5h;

Reference yield:

3-iodo-N<sub>2</sub>-isopropyl-N<sub>1</sub>-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide
666746-35-6

3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide

2,2,2-trifluoroacetaldehyde oxime
819-03-4

2,2,2-trifluoroacetaldehyde oxime

3-iodo-N<sub>2</sub>-isopropyl-N<sub>1</sub>-[2-methyl-4-(3,5-bistrifluoromethyl-4,5-dihydroisoxazol-5-yl)-phenyl]phthalic diamide

3-iodo-N2-isopropyl-N1-[2-methyl-4-(3,5-bistrifluoromethyl-4,5-dihydroisoxazol-5-yl)-phenyl]phthalic diamide

Guidance literature:
2,2,2-trifluoroacetaldehyde oxime; With N-chloro-succinimide; In 1,2-dimethoxyethane; at 40 ℃; for 1h;
3-iodo-N2-isopropyl-N1-[2-methyl-4-(1-trifluoromethylethenyl)phenyl]phthalic diamide; With water; potassium hydrogencarbonate; at 20 ℃; for 5h;
upstream raw materials:

2-methyl-4-(1-trifluoromethylethenyl)aniline

3-iodo-N-isopropylphthalamidic acid

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