(-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

Base Information

Chemical Name:(-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine
CAS No.:316813-39-5
Molecular Formula:C₁₇H₁₉NO₃S
Molecular Weight:317.409
Hs Code.:

Synonyms:(-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

Suppliers and Price of (-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

There total 5 articles about (-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 106-95-6
allyl bromide

: 316813-32-8
(+)-(4R)-4-amino-3-phenylsulfonyl-4-(2-furyl)-2(E)-butene

: 316813-39-5
(-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

Guidance literature:: With potassium carbonate; In acetonitrile; at 0 - 20 ℃;
DOI:10.1016/S0040-4039(00)01423-4

Reference yield:

: 16212-05-8
(allylsulfonyl)benzene

: 316813-39-5
(-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: iPr₂NH; n-BuLi / tetrahydrofuran; hexane / 0.03 h / -100 °C

1.2: 68 percent / TFA / methanol / 2 h / 0 °C

2.1: 90 percent / tert-BuOK / tetrahydrofuran / 2 h / 0 °C

3.1: 78 percent / K₂CO₃ / acetonitrile / 72 h / 0 - 20 °C

With n-butyllithium; potassium tert-butylate; potassium carbonate; diisopropylamine; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1016/S0957-4166(02)00033-2

Reference yield:

: 188447-80-5
(S,E)-4-methyl-N-(2-furylmethylidene)benzenesulfinamide

: 316813-39-5
(-)-(4R)-N-(2-propenyl)-3-phenylsulfonyl-4-(2-furyl)-2(E)-butenyl amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: iPr₂NH; n-BuLi / tetrahydrofuran; hexane / 0.03 h / -100 °C

1.2: 68 percent / TFA / methanol / 2 h / 0 °C

2.1: 90 percent / tert-BuOK / tetrahydrofuran / 2 h / 0 °C

3.1: 78 percent / K₂CO₃ / acetonitrile / 72 h / 0 - 20 °C

With n-butyllithium; potassium tert-butylate; potassium carbonate; diisopropylamine; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1016/S0957-4166(02)00033-2