(1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal

Base Information

Chemical Name:(1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal
CAS No.:102521-17-5
Molecular Formula:C₃₄H₄₈O₄
Molecular Weight:520.753
Hs Code.:

Synonyms:(1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal

Suppliers and Price of (1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of (1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal

There total 13 articles about (1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 102521-15-3,102572-88-3,110716-98-8
(E)-cyclopentadec-2-en-1-one cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: 102521-17-5,102572-90-7,110717-04-9
C₃₄H₄₈O₄

Guidance literature:: With zinc copper; diiodomethane; iodine; potassium carbonate; In diethyl ether; for 24h; Heating;
DOI:10.1021/jo00281a044

Reference yield: 88.0%

: 75-11-6
diiodomethane

: 102521-15-3
(E)-cyclopentadec-2-en-1-one 1,4-di-O-benzyl-D-threitol ketal

: 102521-17-5
(1S,15S)-bicyclo<13.1.0>hexadecan-2-one 1,4-di-O-benzyl-D-threitol ketal

Guidance literature:: With iodine; copper; potassium carbonate; zinc; In diethyl ether; for 4h;
DOI:10.1021/jo00364a019

Reference yield:

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

: 102521-17-5,102572-90-7,110717-04-9
(1R,15R)-bicyclo<13.1.0>hexadecan-2-one cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate

2: zinc-copper couple, potassium carbonate / iodine / diethyl ether / 0.5 h / Heating

With zinc copper; potassium carbonate; iodine; pyridinium p-toluenesulfonate; In diethyl ether;
DOI:10.1016/S0040-4020(01)90002-X