2,3,5-trichlorobenzenecarbothiamide

Base Information

• Chemical Name: 2,3,5-trichlorobenzenecarbothiamide
• CAS No.: 1018688-04-4
• Molecular Formula: C₇H₄Cl₃NS
• Molecular Weight: 240.54
• Mol file: 1018688-04-4.mol

Synonyms:2,3,5-trichlorobenzenecarbothiamide

Chemical Property of 2,3,5-trichlorobenzenecarbothiamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,5-trichlorobenzenecarbothiamide

There total 1 articles about 2,3,5-trichlorobenzenecarbothiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

2,3,5-trichlorobenzamide (50834-09-8) → 2,3,5-trichlorobenzenecarbothiamide (1018688-04-4)

Guidance literature:

With diphosphorus pentasulfide; In tetrahydrofuran; at 50 - 55 ℃; for 4h;

DOI:10.1016/j.ejmech.2007.03.014

Reference yield: 86.0%

2,3,5-trichlorobenzenecarbothiamide (1018688-04-4) + 2-Bromo-4'-phenylacetophenone (135-73-9) → C21H12Cl3NS (1018688-08-8)

Guidance literature:

In methanol; for 4h; Heating;

DOI:10.1016/j.ejmech.2007.03.014

Reference yield: 86.0%

2,3,5-trichlorobenzenecarbothiamide (1018688-04-4) + 4-chlorobenzoylmethyl bromide (536-38-9) → C15H7Cl4NS (1018688-11-3)

Guidance literature:

In methanol; for 4h; Heating;

DOI:10.1016/j.ejmech.2007.03.014

upstream raw materials:

2,3,5-trichlorobenzamide

Downstream raw materials:

C₁₅H₇Cl₃N₂O₂S

C₂₁H₁₂Cl₃NS

4-chloromethyl-2-(2,3,5-trichlorophenyl)-1,3-thiazole

C₁₅H₇Cl₄NS

Refernces