3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone

Base Information

Chemical Name:3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone
CAS No.:267896-58-2
Molecular Formula:C₂₄H₂₁N₅O₄
Molecular Weight:443.462
Hs Code.:

Synonyms:3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone

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Technology Process of 3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone

There total 3 articles about 3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 14484-84-5
3-(4-methoxyphenyl)-4-formylsydnone

: 267896-40-2
4-(4-methylphenyl)-2-phenylsemicarbazide

: 267896-58-2
3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone

Guidance literature:: With sulfuric acid; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1002/jccs.200000027

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 267896-58-2
3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃N / ethyl acetate / 2 h / 20 °C

2: 90 percent / H₂SO₄ / tetrahydrofuran / 1.5 h / 20 °C

With sulfuric acid; triethylamine; In tetrahydrofuran; ethyl acetate; 1: Condensation / 2: Condensation;
DOI:10.1002/jccs.200000027

Reference yield:

: α-chloroformyl phenylhydrazine hydrochloride

: 267896-58-2
3-(4-methoxyphenyl)-sydnon-4-ylaldehyde 2-phenyl-4-(4-methylphenyl)semicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃N / ethyl acetate / 2 h / 20 °C

2: 90 percent / H₂SO₄ / tetrahydrofuran / 1.5 h / 20 °C

With sulfuric acid; triethylamine; In tetrahydrofuran; ethyl acetate; 1: Condensation / 2: Condensation;
DOI:10.1002/jccs.200000027