tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate

Base Information

Chemical Name:tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate
CAS No.:1160241-95-1
Molecular Formula:C₁₇H₂₄N₂O₄S
Molecular Weight:352.455
Hs Code.:

Synonyms:tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate

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Chemical Property of tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate

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Technology Process of tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate

There total 2 articles about tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134360-52-4
N-(t-butyloxycarbonyl)-N'-(p-toluenesulfonyl)ethylenediamine

: 106-96-7
propargyl bromide

: 1160241-95-1
tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate

Guidance literature:: N-(t-butyloxycarbonyl)-N'-(p-toluenesulfonyl)ethylenediamine; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

propargyl bromide; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol900730w

Reference yield:

: 134360-52-4
N-(t-butyloxycarbonyl)-N'-(p-toluenesulfonyl)ethylenediamine

: 106-96-7
propargyl bromide

: 1160241-95-1
tert-butyl 2-(4-methyl-N-(prop-2-ynyl)-phenylsulfonamido)ethylcarbamate

: N-(tert-butoxycarbonyl)-N’-tosyl-(1,2-propadienyl)ethylen-1,2-diamine

Guidance literature:: N-(t-butyloxycarbonyl)-N'-(p-toluenesulfonyl)ethylenediamine; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

propargyl bromide; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/adsc.201400776