Technology Process of Benzeneacetic acid, 5-amino-2-carboxy- (9CI)
There total 5 articles about Benzeneacetic acid, 5-amino-2-carboxy- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
at 20 ℃;
for 3h;
under 2250.23 Torr;
DOI:10.1016/j.bmc.2011.10.058
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium methylate; copper(I) bromide / 100 °C / Inert atmosphere
1.2: pH 1
2.1: sodium hydroxide / methanol / 20 °C / Inert atmosphere
2.2: pH 1 / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 2250.23 Torr
With
palladium 10% on activated carbon; hydrogen; sodium methylate; copper(I) bromide; sodium hydroxide;
In
methanol; ethanol;
DOI:10.1016/j.bmc.2011.10.058
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydroxide / methanol / 20 °C / Inert atmosphere
1.2: pH 1 / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 2250.23 Torr
With
palladium 10% on activated carbon; hydrogen; sodium hydroxide;
In
methanol; ethanol;
DOI:10.1016/j.bmc.2011.10.058
