Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester

Base Information

Chemical Name:Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester
CAS No.:134641-71-7
Molecular Formula:C₁₈H₂₃NO₇S
Molecular Weight:397.449
Hs Code.:

Synonyms:Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester

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Technology Process of Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester

There total 3 articles about Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 134641-70-6
((6S,7R)-7-Nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-phenylsulfanyl-acetic acid ethyl ester

: 134641-71-7
Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester

Guidance literature:: With sodium periodate; In methanol; water; 1.) 0 deg C, 12 h 2.) room temp., 5 h;
DOI:10.1016/S0040-4020(01)96113-7

Reference yield:

: 7605-25-6
ethyl phenylsulfenylacetate

: 134641-71-7
Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, room temp., 30 min 2.) THF, room temp., 2 h

2: 98 percent / sodium metaperiodate / H₂O; methanol / 1.) 0 deg C, 12 h 2.) room temp., 5 h

With sodium periodate; sodium hydride; In methanol; water;
DOI:10.1016/S0040-4020(01)96113-7

Reference yield:

: 103724-93-2
3-nitrocyclohex-2-en-1-one ethylene acetal

: 134641-71-7
Benzenesulfinyl-((6S,7R)-7-nitro-1,4-dioxa-spiro[4.5]dec-6-yl)-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, room temp., 30 min 2.) THF, room temp., 2 h

2: 98 percent / sodium metaperiodate / H₂O; methanol / 1.) 0 deg C, 12 h 2.) room temp., 5 h

With sodium periodate; sodium hydride; In methanol; water;
DOI:10.1016/S0040-4020(01)96113-7