1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene

Base Information

Chemical Name:1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene
CAS No.:748151-57-7
Molecular Formula:C₂₃H₃₀O₆S
Molecular Weight:434.554
Hs Code.:

Synonyms:1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene

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Chemical Property of 1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene

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Technology Process of 1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene

There total 6 articles about 1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 59830-48-7
(2E)-1-p-toluenesulfonyl-2-methyl-4-chloride-2-butene

: 35896-58-3
2,3,4,5-tetramethoxytoluene

: 748151-57-7
1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene

Guidance literature:: With [Etpy]BF₄-ZnCl₂; at 60 ℃; for 0.0416667h; Microwave irradiation; Neat (no solvent);
DOI:10.3390/molecules15129486

Reference yield: 58.8%

: 59830-38-5
(2E)-1-p-toluenesulfonyl-2-methyl-4-hydroxy-2-butene

: 35896-58-3
2,3,4,5-tetramethoxytoluene

: 748151-57-7
1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene

Guidance literature:: With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 80 ℃;
DOI:10.3390/molecules16054097

Reference yield:

: 78-79-5,9003-31-0
isoprene

: 748151-57-7
1-[(E)-3-methyl-4-benzenesulfonyl-3-methylbut-2-enyl]-2,3,4,5-tetramethoxy-6-methylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine hydrochloride; copper(l) chloride / acetonitrile / 6 h / 90 °C / Inert atmosphere

2: sodium acetate / 5 h / 120 °C

3: sodium carbonate / methanol / 0 °C

4: boron trifluoride diethyl etherate / 1,2-dichloro-ethane / 80 °C

With boron trifluoride diethyl etherate; sodium acetate; triethylamine hydrochloride; sodium carbonate; copper(l) chloride; In methanol; 1,2-dichloro-ethane; acetonitrile; 4: Friedel Crafts reaction;
DOI:10.3390/molecules16054097