Technology Process of C30H40N2O8S2
There total 7 articles about C30H40N2O8S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 100 percent / 6 N aq. HCl / 130 °C
2: 90 percent / SOCl2
3: 79 percent / dimethylformamide
4: 48 percent / NaBH4 / ethanol; H2O / 4 h / 50 °C
5: 56 percent / PPh3, diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature
6: 1.) 1 N NaOH, 2.) I2 / 1.) EtOH, a) 0 deg C, 30 min, b) RT, 3 h, 2.) EtOH
With
hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; di-isopropyl azodicarboxylate; iodine; triphenylphosphine;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00035a014
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / SOCl2
2: 79 percent / dimethylformamide
3: 48 percent / NaBH4 / ethanol; H2O / 4 h / 50 °C
4: 56 percent / PPh3, diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature
5: 1.) 1 N NaOH, 2.) I2 / 1.) EtOH, a) 0 deg C, 30 min, b) RT, 3 h, 2.) EtOH
With
sodium hydroxide; sodium tetrahydroborate; thionyl chloride; di-isopropyl azodicarboxylate; iodine; triphenylphosphine;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00035a014
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 56 percent / PPh3, diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature
2: 1.) 1 N NaOH, 2.) I2 / 1.) EtOH, a) 0 deg C, 30 min, b) RT, 3 h, 2.) EtOH
With
sodium hydroxide; di-isopropyl azodicarboxylate; iodine; triphenylphosphine;
In
tetrahydrofuran;
DOI:10.1021/jm00035a014