(3R)-(-)-3-(1-Methyl-1H-indol-3-YL)-1-butanol

Base Information

Chemical Name:(3R)-(-)-3-(1-Methyl-1H-indol-3-YL)-1-butanol
CAS No.:406920-66-9
Molecular Formula:C₁₃H₁₇NO
Molecular Weight:203.284
Hs Code.:
European Community (EC) Number:631-026-6
Nikkaji Number:J3.061.006G
Mol file:406920-66-9.mol

Synonyms:(3R)-(-)-3-(1-METHYL-1H-INDOL-3-YL)-1-BUTANOL;(R)-3-(1-Methyl-1H-indol-3-yl)butan-1-ol;(3R)-3-(1-methylindol-3-yl)butan-1-ol;406920-66-9;(3R)-3-(1-methyl-1H-indol-3-yl)butan-1-ol

Suppliers and Price of (3R)-(-)-3-(1-Methyl-1H-indol-3-YL)-1-butanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
(3R)-(?)-3-(1-Methyl-1H-indol-3-yl)-1-butanol Aldrich
100mg
$ 55.10

American Custom Chemicals Corporation
(3R)-(-)-3-(1-METHYL-1H-INDOL-3-YL)-1-BUTANOL 95.00%
5MG
$ 501.96

Total 1 raw suppliers

Chemical Property of (3R)-(-)-3-(1-Methyl-1H-indol-3-YL)-1-butanol

Chemical Property:

Refractive Index:n20/D 1.5860(lit.)
Boiling Point:325-326 °C(lit.)
Flash Point:>230 °F
Density:1.109 g/mL at 25 °C(lit.)
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:203.131014166
Heavy Atom Count:15
Complexity:207

Purity/Quality:: (3R)-(?)-3-(1-Methyl-1H-indol-3-yl)-1-butanol Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22-37/38-41-42/43
Safety Statements: 26-36

MSDS Files:

Useful:

Canonical SMILES:CC(CCO)C1=CN(C2=CC=CC=C21)C
Isomeric SMILES:C[C@H](CCO)C1=CN(C2=CC=CC=C21)C

Technology Process of (3R)-(-)-3-(1-Methyl-1H-indol-3-YL)-1-butanol

There total 7 articles about (3R)-(-)-3-(1-Methyl-1H-indol-3-YL)-1-butanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-3-(1-methyl-1H-indol-3-yl)-butanal

: 406920-76-1,406920-66-9
C₁₃H₁₇NO

Guidance literature:: With sodium tetrahydroborate; In methanol; toluene; at -40 - 0 ℃; optical yield given as %ee;
DOI:10.1055/s-0029-1217552

Reference yield:

: 603-76-9
1-methylindole

: 406920-76-1,406920-66-9
C₁₃H₁₇NO

Guidance literature:: Multi-step reaction with 2 steps

1: camphor sulphonyl hydrazine; trifluoroacetic acid / toluene / 9 h / -40 °C

2: sodium tetrahydroborate / methanol; toluene / -40 - 0 °C

With sodium tetrahydroborate; camphor sulphonyl hydrazine; trifluoroacetic acid; In methanol; toluene; 1: Friedel Crafts alkylation;
DOI:10.1055/s-0029-1217552