4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt

Base Information

Chemical Name:4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt
CAS No.:1450916-07-0
Molecular Formula:C₂HF₃O₂*C₁₄H₁₇N₃O₄
Molecular Weight:405.331
Hs Code.:

Synonyms:4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt

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Chemical Property of 4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt

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Technology Process of 4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt

There total 3 articles about 4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1450915-98-6
4-{4-[(R)-5-[(((4-fluorophenyl)methylene)amino)methyl]-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one

: 76-05-1
trifluoroacetic acid

: 1450916-07-0
4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt

Guidance literature:: With water; In ethanol; at -15 - 65 ℃; for 1h;

Reference yield:

: 1313613-18-1
[4-(3-oxo-morpholin-4-yl)phenyl]carbamic acid benzyl ester

: 1450916-07-0
4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium tert-butoxide / dichloromethane / 0.17 h / 40 °C

1.2: 18 h / 35 - 45 °C

2.1: water / ethanol / 1 h / -15 - 65 °C

With water; lithium tert-butoxide; In ethanol; dichloromethane;

Reference yield:

: 1450915-96-4
isobutyl 4-(3-oxomorpholin-4-yl)phenylcarbamate

: 1450916-07-0
4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium tert-butoxide / dichloromethane / 0.17 h / 40 °C

1.2: 17 h / 35 - 45 °C

2.1: water / ethanol / 1 h / -15 - 65 °C

With water; lithium tert-butoxide; In ethanol; dichloromethane;