(2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone

Base Information

• Chemical Name: (2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone
• CAS No.: 1071461-48-7
• Molecular Formula: C₃₆H₃₇NO₅
• Molecular Weight: 563.693

Synonyms:(2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone

Chemical Property of (2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone

Chemical Property:

Purity/Quality:

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Technology Process of (2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone

There total 1 articles about (2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanol → (2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone (1071461-48-7)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1016/j.tet.2008.07.089

Reference yield: 92.1%

(2S,4S,5R)-5-[N-benzyl-N-(benzyloxycarbonyl)amino]-2,4-dibenzyloxycycloheptanone (1071461-48-7) → calystegine A7 (197565-90-5)

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; In ethyl acetate; for 24h; under 1808.92 Torr;

DOI:10.1016/j.tet.2008.07.089

Downstream raw materials:

calystegine A₇

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