Carbamothioic acid, methyl-, O-2-cyclohepten-1-yl ester (9CI)

Base Information

Chemical Name:Carbamothioic acid, methyl-, O-2-cyclohepten-1-yl ester (9CI)
CAS No.:405238-01-9
Molecular Formula:C₉H₁₅NOS
Molecular Weight:185.29
Hs Code.:
Mol file:405238-01-9.mol

Synonyms:Carbamothioic acid, methyl-, O-2-cyclohepten-1-yl ester (9CI)

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Chemical Property of Carbamothioic acid, methyl-, O-2-cyclohepten-1-yl ester (9CI)

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Technology Process of Carbamothioic acid, methyl-, O-2-cyclohepten-1-yl ester (9CI)

There total 5 articles about Carbamothioic acid, methyl-, O-2-cyclohepten-1-yl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 79605-67-7,4096-38-2
2-cycloheptenol

: 556-61-6
methyl thioisocyanate

: 405238-01-9
(+/-)-methylthiocarbamic acid O-(cyclohept-2-enyl) ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/jo010668b

Reference yield:

: 405238-01-9
(+/-)-methylthiocarbamic acid O-(cyclohept-2-enyl) ester

: 405238-01-9
methylthiocarbamic acid S-((S)-cyclohept-2-enyl) ester

: 405238-01-9
methylthiocarbamic acid S-((R)-cyclohept-2-enyl) ester

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (+)-(1R,2R)-o-C₆H₄(NHCOC₆H₄PPh₂-o)2; In dichloromethane; at 20 ℃; for 5h; Title compound not separated from byproducts.;
DOI:10.1021/jo010668b

Reference yield:

: 405238-01-9
(+/-)-methylthiocarbamic acid O-(cyclohept-2-enyl) ester

: 405238-01-9
methylthiocarbamic acid S-((S)-cyclohept-2-enyl) ester

: 405238-01-9
methylthiocarbamic acid S-((R)-cyclohept-2-enyl) ester

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (+)-(1R,2R)-o-C₆H₄(NHCOC₆H₄PPh₂-o)2; In dichloromethane; at 20 ℃; for 5h; Title compound not separated from byproducts.;
DOI:10.1021/jo010668b