1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene

Base Information

Chemical Name:1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene
CAS No.:142362-68-3
Molecular Formula:C₁₂H₁₇N₇
Molecular Weight:259.314
Hs Code.:

Synonyms:1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene

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Chemical Property of 1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene

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Technology Process of 1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene

There total 1 articles about 1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 624-90-8
methyl azide

: 139688-58-7
1,4-Dimethyl-5-(1-phenylethyl)tetrazolium-trifluormethansulfonat

: 142362-68-3
1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene

Guidance literature:: 1,4-Dimethyl-5-(1-phenylethyl)tetrazolium-trifluormethansulfonat; With sodium hydride; In diethyl ether; for 3h;

methyl azide; In diethyl ether; at 5 ℃; for 120h;
DOI:10.1002/hlca.200590126

Reference yield:

: 142362-68-3
1,4,6,9-tetramethyl-9-phenyl-1,2,3,4,6,7,8-heptaazaspiro[4.4]nona-2,7-diene

: 10557-01-4
(E)-N-(α-methylbenzylidene)methylamine

: 140111-27-9
[1,3-Dimethyl-3-phenyl-aziridin-(2E)-ylidene]-methyl-amine

: 142362-70-7
[3,5-Dimethyl-5-phenyl-3,5-dihydro-[1,2,3]triazol-(4Z)-ylidene]-methyl-amine

: 75-05-8,26809-02-9
acetonitrile

Guidance literature:: In benzene-d6; at 130 ℃; for 10h; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;