1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene

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Chemical Name:1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene
CAS No.:1234908-61-2
Molecular Formula:C₂₈H₁₉BrF₆OS₂
Molecular Weight:629.485
Hs Code.:

Synonyms:1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene

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Chemical Property of 1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene

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Technology Process of 1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene

There total 1 articles about 1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 938459-33-7
3-(2-(5-chloro-2-methylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-5-(4-methoxyphenyl)-2-methylthiophene

: 589-87-7
1,4-bromoiodobenzene

: 1234908-61-2
1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene

Guidance literature:: 3-(2-(5-chloro-2-methylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-5-(4-methoxyphenyl)-2-methylthiophene; With n-butyllithium; In diethyl ether; hexane; at 20 ℃;

With boric acid tributyl ester; In diethyl ether; hexane; at 20 ℃; for 1h;

1,4-bromoiodobenzene; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; for 16h; Reflux;
DOI:10.1002/asia.200900503

Reference yield: 76.0%

: 1234908-61-2
1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene

: 1-(4-ethynylphenyl)-3,5,7-tris-(4-carboethoxyphenyl)adamantane

: C₆₇H₅₈F₆O₇S₂

Guidance literature:: 1-[5-(4-methoxyphenyl)-2-methylthienyl-3-yl]-2-[2-methyl-5-(4-bromophenyl)-thien-3-yl]-3,3,4,4,5,5-hexafluorocyclopentene; With PdCl₂(MeCN)₂; K₃PO₄; XPhos; In acetonitrile; for 30h; Inert atmosphere;

1-(4-ethynylphenyl)-3,5,7-tris-(4-carboethoxyphenyl)adamantane; In acetonitrile; at 80 ℃; for 4h; Inert atmosphere;
DOI:10.1002/asia.200900503