phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
CAS No.:129253-68-5
Molecular Formula:C₂₆H₂₅Br₂NO₁₁
Molecular Weight:687.293
Hs Code.:

Synonyms:phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

There total 3 articles about phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.7%

: 5415-23-6
2,6-dibromophenolindophenol sodium salt

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 129253-68-5
phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With silver(l) oxide; In acetonitrile; at 40 ℃;
DOI:10.1248/cpb.38.13

Reference yield: 8.8%

: 2582-33-4
2,6-dibromophenolindophenol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 129273-03-6
2,6-dibromophenolindophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 129253-68-5
phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: With silver(l) oxide; In benzene; Heating;
DOI:10.1248/cpb.38.13

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 129253-68-5
phenolindo-3',5'-dibromophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93.5 percent / PBr₃, H₂O / CH₂Cl₂ / 10 h / 30 °C

2: 8.8 percent / Ag₂O / benzene / Heating

With water; phosphorus tribromide; silver(l) oxide; In dichloromethane; benzene;
DOI:10.1248/cpb.38.13