C₅₄H₃₆N₂

Base Information

Chemical Name:C₅₄H₃₆N₂
CAS No.:1421701-41-8
Molecular Formula:C₅₄H₃₆N₂
Molecular Weight:712.893
Hs Code.:

C<sub>54</sub>H<sub>36</sub>N<sub>2</sub>

Synonyms:C₅₄H₃₆N₂

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Chemical Property of C₅₄H₃₆N₂

Chemical Property:

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Technology Process of C₅₄H₃₆N₂

There total 7 articles about C₅₄H₃₆N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 897671-81-7
N-phenyl-[1,1':4',1-terphenyl]-4-amine

: 1421701-40-7
C₃₀H₁₈BrN

: 1421701-41-8
C₅₄H₃₆N₂

Guidance literature:: With bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; XPhos; In 5,5-dimethyl-1,3-cyclohexadiene; at 120 ℃; for 3h; Inert atmosphere;

Reference yield:

: 6286-72-2
9-(2-nitrophenyl)-9H-carbazole

: 1421701-41-8
C₅₄H₃₆N₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: stannous chloride dihydrate / ethanol / 8 h / 70 °C / Inert atmosphere

1.2: 1 h / 20 °C

2.1: sulfuric acid; sodium nitrite / water; acetic acid / 0.75 h / 10 - 130 °C / Cooling with ice

3.1: N-Bromosuccinimide / dichloromethane / 1 h / 20 °C

3.2: 13 h

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane; toluene / 17 h / 120 °C / Inert atmosphere

5.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; 1,4-dioxane / 9 h / 100 °C / Inert atmosphere

6.1: sodium t-butanolate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; N-Bromosuccinimide; stannous chloride dihydrate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sulfuric acid; potassium acetate; potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; sodium nitrite; XPhos; In 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane; water; acetic acid; toluene;

Reference yield:

: 205-95-8
indolo<3,2,1-jk>carbazole

: 1421701-41-8
C₅₄H₃₆N₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-Bromosuccinimide / dichloromethane / 1 h / 20 °C

1.2: 13 h

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane; toluene / 17 h / 120 °C / Inert atmosphere

3.1: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / water; 1,4-dioxane / 9 h / 100 °C / Inert atmosphere

4.1: sodium t-butanolate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; XPhos / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 120 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; N-Bromosuccinimide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; sodium t-butanolate; XPhos; In 1,4-dioxane; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; toluene;