methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate

Base Information

Chemical Name:methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate
CAS No.:227286-89-7
Molecular Formula:C₃₀H₂₅NO₄
Molecular Weight:463.533
Hs Code.:

methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-<N-(9-phenylfluoren-9-yl)amino>propanoate

Synonyms:methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate

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Technology Process of methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate

There total 4 articles about methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 227286-96-6
methyl (S)-2--3-<3,4-bis(tert-butyldimethylsilyloxy)phenyl>propanoate

: 227286-89-7
methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate

Guidance literature:: With cesium fluoride; In dichloromethane; N,N-dimethyl-formamide; at 110 ℃; for 1h;
DOI:10.1016/S0040-4020(99)00133-7

Reference yield:

: 55135-66-5
9-bromo-9-phenyl-9H-fluorene

: 227286-89-7
methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / triethylamine, lead nitrate / CH₂Cl₂ / 72 h / Ambient temperature

2: 85 percent / cesium fluoride / dimethylformamide; CH₂Cl₂ / 1 h / 110 °C

With lead(II) nitrate; triethylamine; cesium fluoride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(99)00133-7

Reference yield:

: 1421-65-4
L-dopa methyl ester hydrochloride

: 227286-89-7
methyl (S)-3-<3,4-(methylenedioxy)phenyl>-2-propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / imidazole / dimethylformamide / 3.5 h

2: 82 percent / triethylamine, lead nitrate / CH₂Cl₂ / 72 h / Ambient temperature

3: 85 percent / cesium fluoride / dimethylformamide; CH₂Cl₂ / 1 h / 110 °C

With 1H-imidazole; lead(II) nitrate; triethylamine; cesium fluoride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(99)00133-7