ba-D-Gulofuranosiduronic acid, methyl 5-amino-5-deoxy-5-C-methyl- (9CI)

Base Information

Chemical Name:ba-D-Gulofuranosiduronic acid, methyl 5-amino-5-deoxy-5-C-methyl- (9CI)
CAS No.:360577-35-1
Molecular Formula:C₈H₁₅NO₆
Molecular Weight:221.21
Hs Code.:
Mol file:360577-35-1.mol

Synonyms:bta-D-Gulofuranosiduronicacid,methyl5-amino-5-deoxy-5-C-methyl-(9CI);ba-D-Gulofuranosiduronic acid, methyl 5-amino-5-deoxy-5-C-methyl- (9CI)

Suppliers and Price of ba-D-Gulofuranosiduronic acid, methyl 5-amino-5-deoxy-5-C-methyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of ba-D-Gulofuranosiduronic acid, methyl 5-amino-5-deoxy-5-C-methyl- (9CI)

Chemical Property:

PSA：122.24000
LogP:-1.41820

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ba-D-Gulofuranosiduronic acid, methyl 5-amino-5-deoxy-5-C-methyl- (9CI)

There total 3 articles about ba-D-Gulofuranosiduronic acid, methyl 5-amino-5-deoxy-5-C-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 360577-34-0
(5'S)-5'-methyl-5'-[methyl (4R)-β-D-erythrofuranosid-4-C-yl]-imidazolidin-2',4'-dione

: 360577-35-1,360577-31-7,360577-37-3
methyl (5S)-5-amino-5-C-carboxy-5,6-dideoxy-α-L-lyxo-hexofuranoside

Guidance literature:: With barium dihydroxide; In water; for 6h; Heating;
DOI:10.1016/S0008-6215(01)00109-4

Reference yield:

: 63803-17-8
methyl 6-deoxy-2,3-O-isopropylidene-α-L-lyxo-hexofuranosid-5-ulose

: 360577-35-1,360577-31-7,360577-37-3
methyl (5S)-5-amino-5-C-carboxy-5,6-dideoxy-α-L-lyxo-hexofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / (NH₄)2CO₃ / ethanol / 6 h / 60 °C

2: 66 percent / AcOH / H₂O / 1.25 h / 80 °C

3: 40 percent / barium hydroxyde octahydrate / H₂O / 6 h / Heating

With barium dihydroxide; ammonium carbonate; acetic acid; In ethanol; water;
DOI:10.1016/S0008-6215(01)00109-4

Reference yield:

: 360577-32-8
(5'S)-5'-methyl-5'-[methyl (4R)-2,3-O-isopropylidene-β-D-erythrofuranosid-4-C-yl]-imidazolidin-2',4'-dione

: 360577-35-1,360577-31-7,360577-37-3
methyl (5S)-5-amino-5-C-carboxy-5,6-dideoxy-α-L-lyxo-hexofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / AcOH / H₂O / 1.25 h / 80 °C

2: 40 percent / barium hydroxyde octahydrate / H₂O / 6 h / Heating

With barium dihydroxide; acetic acid; In water;
DOI:10.1016/S0008-6215(01)00109-4