Bicyclo[2.2.1]heptan-2-ol, 1-[(dimethylamino)methyl]-7,7-dimethyl-, (1S,2S,4S)- (9CI)

Base Information

Chemical Name:Bicyclo[2.2.1]heptan-2-ol, 1-[(dimethylamino)methyl]-7,7-dimethyl-, (1S,2S,4S)- (9CI)
CAS No.:360554-66-1
Molecular Formula:C₁₂H₂₃NO
Molecular Weight:197.321
Hs Code.:
Mol file:360554-66-1.mol

Synonyms:Bicyclo[2.2.1]heptan-2-ol, 1-[(dimethylamino)methyl]-7,7-dimethyl-, (1S,2S,4S)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[2.2.1]heptan-2-ol, 1-[(dimethylamino)methyl]-7,7-dimethyl-, (1S,2S,4S)- (9CI)

Chemical Property:

PSA：23.47000
LogP:1.73520

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of Bicyclo[2.2.1]heptan-2-ol, 1-[(dimethylamino)methyl]-7,7-dimethyl-, (1S,2S,4S)- (9CI)

There total 4 articles about Bicyclo[2.2.1]heptan-2-ol, 1-[(dimethylamino)methyl]-7,7-dimethyl-, (1S,2S,4S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 851512-56-6
N,N,7,7-tetramethyl-2-oxobicyclo[2.2.1]heptane-1-carboxamide

: 360554-66-1
(1R,2R)-10-(dimethylamino)isoborneol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2.5h;
DOI:10.1055/s-2005-861788

Reference yield:

: 464-78-8,6994-94-1,64234-14-6,40724-67-2
(1S)-(+)-ketopinic acid

: 360554-66-1
(1R,2R)-10-(dimethylamino)isoborneol

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: 1.10 g / tetrahydrofuran; H₂O / 1 h / 20 °C

3: 92 percent / LiAlH₄ / tetrahydrofuran / 2.5 h

With lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; water;
DOI:10.1055/s-2005-861788

Reference yield:

: 54371-12-9,66884-33-1,66965-39-7,86023-72-5
ketopinic acid chloride

: 360554-66-1
(1R,2R)-10-(dimethylamino)isoborneol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.10 g / tetrahydrofuran; H₂O / 1 h / 20 °C

2: 92 percent / LiAlH₄ / tetrahydrofuran / 2.5 h

With lithium aluminium tetrahydride; In tetrahydrofuran; water;
DOI:10.1055/s-2005-861788