1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane

Base Information

Chemical Name:1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane
CAS No.:110464-20-5
Molecular Formula:C₂₁H₂₅Cl₂NO₇
Molecular Weight:474.338
Hs Code.:

Synonyms:1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane

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Chemical Property of 1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane

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Technology Process of 1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane

There total 2 articles about 1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 638-07-3
ethyl (2-chloroaceto)acetate

: 110464-20-5
1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, 2.) RT, 16 h

2: 7 percent / ethanol / 16 h / Heating

3: 55 percent / aq. HOAc / 72 h / Ambient temperature

With sodium hydride; acetic acid; In ethanol;
DOI:10.1021/jm00105a004

Reference yield:

: 110464-45-4
4-(2,2-Dimethyl-[1,3]dioxolan-4-ylmethoxy)-3-oxo-butyric acid ethyl ester

: 110464-20-5
1-{[4-(2,3-dichlorophenyl)-3-ethoxycarbonyl-5-methoxycarbonyl-6-methyl-1,4-dihydropyrid-2-yl]methoxy}-2,3-dihydroxypropane

Guidance literature:: Multi-step reaction with 2 steps

1: 7 percent / ethanol / 16 h / Heating

2: 55 percent / aq. HOAc / 72 h / Ambient temperature

With acetic acid; In ethanol;
DOI:10.1021/jm00105a004