(R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one

Base Information

Chemical Name:(R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one
CAS No.:107707-11-9
Molecular Formula:C₁₉H₂₄O₇
Molecular Weight:364.395
Hs Code.:

Synonyms:(R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one

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Chemical Property of (R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one

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Technology Process of (R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one

There total 3 articles about (R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 98829-07-3
(5R)-5-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-3-hydroxy-4-(methoxymethoxy)-2,5-dihydrofuran-2-one

: 107707-11-9
(R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one

Guidance literature:: With potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide; at 50 ℃; for 3h;
DOI:10.1021/jm00399a019

Reference yield:

: 50-81-7,98966-42-8
ascorbic acid

: 107707-11-9
(R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / acetyl chloride / 18 h / Ambient temperature

2: 52 percent / potassium carbonate / tetrahydrofuran; dimethylformamide / 4 h / Ambient temperature

3: 68 percent / potassium carbonate / tetrahydrofuran; dimethylsulfoxide / 3 h / 50 °C

With potassium carbonate; acetyl chloride; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00399a019

Reference yield:

: 15042-01-0
5,6-O-isopropylidene-L-ascorbic acid

: 107707-11-9
(R)-5-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-4-methoxymethoxy-3-(4-methyl-benzyloxy)-5H-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / potassium carbonate / tetrahydrofuran; dimethylformamide / 4 h / Ambient temperature

2: 68 percent / potassium carbonate / tetrahydrofuran; dimethylsulfoxide / 3 h / 50 °C

With potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00399a019