tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate
CAS No.:1171122-40-9
Molecular Formula:C₁₈H₂₇NO₄
Molecular Weight:321.417
Hs Code.:

Synonyms:tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate

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Chemical Property of tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate

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Technology Process of tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate

There total 10 articles about tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1125824-79-4
tert-butyl-2-phenyltetrahydro-4H-(1,3)dioxino(5,4-b)pyridine-5(4aH)-carboxylate

: 1171122-40-9
tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate

Guidance literature:: With triethylsilane; ethylaluminum dichloride; In dichloromethane; at -78 ℃; for 1h; regioselective reaction;
DOI:10.1016/j.tetlet.2009.03.007

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₁₃H₁₉NO₂

: 1171122-40-9
tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; for 6h;
DOI:10.1016/j.tetlet.2014.09.118

Reference yield:

: (1S,2S,6R)-2-benzyloxy-8-tert-butyloxycarbonyl-6-oxa-8-azabicyclo[3.2.1]octane

: 1171122-40-9
tert-butyl (2S,3S)-3-(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo902324h