N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

Base Information

Chemical Name:N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2
CAS No.:928342-13-6
Molecular Formula:C₅₄H₅₆ClN₉O₁₀
Molecular Weight:1026.55
Hs Code.:

N<sup>α</sup>-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

Synonyms:N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

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Chemical Property of N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

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Technology Process of N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

There total 11 articles about N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₄ClN₅O₃

: 928342-12-5
N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-OH

: 928342-13-6
N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

Guidance literature:: With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2006.12.007

Reference yield:

: C₂₀H₂₁ClN₄O₂

: 928342-13-6
N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

Guidance literature:: Multi-step reaction with 3 steps

1: N,N'-dicyclohexylcarbodiimide; N-hydroxysuccinimide / tetrahydrofuran / 0 - 20 °C

2: hydrochloric acid / ethyl acetate / 2 h / 20 °C

3: N,N'-dicyclohexylcarbodiimide; N-hydroxysuccinimide / tetrahydrofuran / 0 - 20 °C

With hydrogenchloride; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.bmc.2006.12.007

Reference yield:

: 928342-10-3
Boc-Gly-Trp-(p-Cl-Phe)-NH₂

: 928342-13-6
N^α-(N,N'-bis-benzyloxycarbonyl)amidino-Tyr(Me)-D-Pro-Gly-Trp-(p-Cl-Phe)-NH2

Guidance literature:: Multi-step reaction with 2 steps

1: hydrochloric acid / ethyl acetate / 2 h / 20 °C

2: N,N'-dicyclohexylcarbodiimide; N-hydroxysuccinimide / tetrahydrofuran / 0 - 20 °C

With hydrogenchloride; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.bmc.2006.12.007