benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside
CAS No.:77453-60-2
Molecular Formula:C₂₃H₂₅NO₆
Molecular Weight:411.455
Hs Code.:

Synonyms:benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside

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Chemical Property of benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside

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Technology Process of benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside

There total 2 articles about benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 63593-15-7
benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-formyl-α-D-erythro-hex-2-enopyranoside

: 77453-60-2
benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85897-8

Reference yield:

: 62175-13-7
benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-nitromethyl-α-D-erythro-hex-2-enopyranoside

: 77453-60-2
benzyl 2-acetamido-4,6-O-benzylidene-2,3-dideoxy-3-C-hydroxymethyl-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride; 2.) titanium(III) chloride / 1.) DMF, mineral oil, -10 deg C, 45 min; 2.) pH 1

2: 80 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; titanium(III) chloride; sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0008-6215(00)85897-8