3-phenyl-2-triethylsiloxypropiophenone

Base Information

Chemical Name:3-phenyl-2-triethylsiloxypropiophenone
CAS No.:932747-33-6
Molecular Formula:C₂₁H₂₈O₂Si
Molecular Weight:340.538
Hs Code.:

Synonyms:3-phenyl-2-triethylsiloxypropiophenone

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Chemical Property of 3-phenyl-2-triethylsiloxypropiophenone

Chemical Property:

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Technology Process of 3-phenyl-2-triethylsiloxypropiophenone

There total 6 articles about 3-phenyl-2-triethylsiloxypropiophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 932747-23-4
2,3-diphenyl-2-(triethylsiloxy)propanenitrile

: 932747-33-6
3-phenyl-2-triethylsiloxypropiophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / DIBAH / CH₂Cl₂; toluene / 1 h / -78 °C

2: chiral organoaluminum Lewis acid catalyst / toluene / 12 h / -20 °C

With diisobutylaluminium hydride; chiral organoaluminum Lewis acid catalyst; In dichloromethane; toluene;
DOI:10.1021/ja063051q

Reference yield:

: 18301-88-7
triethylsilylcyanide

: 932747-33-6
3-phenyl-2-triethylsiloxypropiophenone

Guidance literature:: Multi-step reaction with 4 steps

1.1: I₂ / CH₂Cl₂ / 0.5 h / 0 °C

2.1: diisopropylamine; n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 2.83 g / tetrahydrofuran; hexane / 3 h / -78 °C

3.1: 100 percent / DIBAH / CH₂Cl₂; toluene / 1 h / -78 °C

4.1: chiral organoaluminum Lewis acid catalyst / toluene / 12 h / -20 °C

With n-butyllithium; iodine; diisobutylaluminium hydride; diisopropylamine; chiral organoaluminum Lewis acid catalyst; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ja063051q

Reference yield:

: 57137-86-7
2-phenyl-2-(triethylsiloxy)acetonitrile

: 932747-33-6
3-phenyl-2-triethylsiloxypropiophenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropylamine; n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 2.83 g / tetrahydrofuran; hexane / 3 h / -78 °C

2.1: 100 percent / DIBAH / CH₂Cl₂; toluene / 1 h / -78 °C

3.1: chiral organoaluminum Lewis acid catalyst / toluene / 12 h / -20 °C

With n-butyllithium; diisobutylaluminium hydride; diisopropylamine; chiral organoaluminum Lewis acid catalyst; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1021/ja063051q