[PdCl(2-bromobenzylidene-2,6-diisopropylphenylamine(-1H)]2

Base Information

Chemical Name:[PdCl(2-bromobenzylidene-2,6-diisopropylphenylamine(-1H)]2
CAS No.:710294-20-5
Molecular Formula:C₃₈H₄₂Br₂Cl₂N₂Pd₂
Molecular Weight:970.319
Hs Code.:

Synonyms:[PdCl(2-bromobenzylidene-2,6-diisopropylphenylamine(-1H)]2

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Chemical Property of [PdCl(2-bromobenzylidene-2,6-diisopropylphenylamine(-1H)]2

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Technology Process of [PdCl(2-bromobenzylidene-2,6-diisopropylphenylamine(-1H)]2

There total 2 articles about [PdCl(2-bromobenzylidene-2,6-diisopropylphenylamine(-1H)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1416955-79-7
(2-bromobenzylidene)(2,6-diisopropylphenyl)amine

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 710294-20-5
[PdCl(2-bromobenzylidene-2,6-diisopropylphenylamine(-1H)]2

Guidance literature:: With sodium acetate; In dichloromethane; (N2); using Schlenk techniques; addn. of 2-bromobenzylidene-2,6-diisopropylphenylamine (1 equiv.) and NaOAc (2 equiv.) to stirring soln. of (MeCN)2PdCl2 (1 equiv.) in CH2Cl2, stirring for 6 h at room temp.; removal of solvent, redissolving in CH2Cl2, filtration, removal of solvent from filtrate, recrystn. from CH2Cl2:hexane;
DOI:10.1016/j.jorganchem.2011.07.044

Reference yield: 76.0%

: 1416955-79-7
(2-bromobenzylidene)(2,6-diisopropylphenyl)amine

: palladium dichloride

: 710294-20-5
(PdCl(BrC₆H₃CHNC₆H₃(CH(CH₃)2)2))2

Guidance literature:: With sodium acetate; In tetrahydrofuran; under N2; pre-dried MeCN added to PdCl2; stirred at room temp. for 2 d; solvent removed to dryness; ligand (1.06 equiv.), Na acetate (15.5 equiv.) and THF added; stirred at room temp. for 38 h; solvent removed; CH2Cl2 added; filtered through Celite; filtrate concd.;washed with hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2004.03.002