3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane

Base Information

Chemical Name:3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane
CAS No.:1610416-83-5
Molecular Formula:C₁₁H₁₂ClFO₂
Molecular Weight:230.666
Hs Code.:

Synonyms:3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane

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Chemical Property of 3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane

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Technology Process of 3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane

There total 2 articles about 3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1610416-82-4
3-(2-chloro-4-(methoxymethyl)phenyl)oxetan-3-ol

: 1610416-83-5
3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane

Guidance literature:: With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 1610416-69-7
1-bromo-2-chloro-4-(methoxymethyl)benzene

: 1610416-83-5
3-(2-chloro-4-(methoxymethyl)phenyl)-3-fluorooxetane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 0.58 h

2.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 1 h / 0 °C

With n-butyllithium; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; hexane; dichloromethane;