2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone

Base Information

Chemical Name:2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone
CAS No.:154317-70-1
Molecular Formula:C₃₁H₄₂N₂O₂S₂Si₃
Molecular Weight:623.075
Hs Code.:

Synonyms:2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone

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Chemical Property of 2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone

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Technology Process of 2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone

There total 1 articles about 2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 148549-36-4
2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal

: 154317-70-1
2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone

Guidance literature:: With hydrogenchloride; In acetonitrile; for 16h; Ambient temperature;
DOI:10.1021/jo00084a049

Reference yield: 24.0%

: 154317-70-1
2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone

: 1-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-1-en-4-yne

Guidance literature:: With lithium hydroxide; In diethyl ether; for 36h; Ambient temperature;
DOI:10.1021/jo00084a049

Reference yield:

: 106-45-6
para-thiocresol

: 154317-70-1
2-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-4-ynal (toluenesulfonyl)hydrazone

: 1-(Phenylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-1-en-4-yne

: 1-(Tolylthio)-3,3-bis<(trimethylsilyl)ethynyl>-5-(trimethylsilyl)pent-1-en-4-yne

Guidance literature:: With lithium hydroxide; In diethyl ether; for 36h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00084a049