bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene

Base Information

Chemical Name:bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene
CAS No.:1283056-72-3
Molecular Formula:C₆₄H₇₂N₂O₁₄S₂
Molecular Weight:1157.41
Hs Code.:

Synonyms:bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene

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Chemical Property of bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene

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Technology Process of bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene

There total 3 articles about bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1283056-71-2
bis[methyl-6-amino-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-p-xylene

: 98-59-9
p-toluenesulfonyl chloride

: 1283056-72-3
bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene

Guidance literature:: With pyridine; at -20 ℃; for 48h;
DOI:10.1016/j.crci.2010.03.032

Reference yield:

: 623-24-5
1,4-bis(bromomethyl)benzene

: 1283056-72-3
bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; sodium hydroxide / water; toluene / 24 h / 80 °C

2: 5%-palladium/activated carbon; triethylamine / methanol; ethyl acetate / 24 h

3: pyridine / 48 h / -20 °C

With pyridine; 5%-palladium/activated carbon; tetrabutylammomium bromide; triethylamine; sodium hydroxide; In methanol; water; ethyl acetate; toluene;
DOI:10.1016/j.crci.2010.03.032

Reference yield:

: 1283056-70-1
bis[methyl-6-azido-2,3-di-O-benzyl-6-deoxy-4-yloxy-α-D-glucopyranoside]-p-xylene

: 1283056-72-3
bis[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-p-xylene

Guidance literature:: Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; triethylamine / methanol; ethyl acetate / 24 h

2: pyridine / 48 h / -20 °C

With pyridine; 5%-palladium/activated carbon; triethylamine; In methanol; ethyl acetate;
DOI:10.1016/j.crci.2010.03.032