(1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

Base Information

Chemical Name:(1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate
CAS No.:1232680-34-0
Molecular Formula:C₄₅H₄₂O₁₀
Molecular Weight:742.822
Hs Code.:

Synonyms:(1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

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Chemical Property of (1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

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Technology Process of (1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

There total 1 articles about (1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1232680-33-9
(1S,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-6-methylcyclohex-2-enyl acetate

: 1232680-34-0
(1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; tert-butyl alcohol; at 0 ℃; for 20h;
DOI:10.1021/ol101009q

Reference yield: 68.0%

: 1232680-34-0
(1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

: 1232680-35-1
(1S,2S,3R,4R,6R)-4-(5,7-dihydroxy-2-(4-hydroxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; ethanol; at -50 - 20 ℃;
DOI:10.1021/ol101009q

Reference yield: 54.0%

: 1445-45-0
Trimethyl orthoacetate

: 1232680-34-0
(1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate

: 1232680-36-2
(1S,2R,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2-hydroxy-6-methylcyclohexane-1,3-diyl diacetate

: 1232680-37-3
(1S,2S,3S,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-3-hydroxy-6-methylcyclohexane-1,2-diyl diacetate

Guidance literature:: Trimethyl orthoacetate; (1S,2S,3R,4R,6R)-4-(5,7-bis(benzyloxy)-2-(4-benzyloxyphenyl)-4-oxo-4H-chromen-3-yl)-2,3-dihydroxy-6-methylcyclohexyl acetate; With toluene-4-sulfonic acid; In dichloromethane; at 0 ℃; for 0.5h;

With water; acetic acid; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1021/ol101009q