C₂₃H₃₁NO₄

Base Information

Chemical Name:C₂₃H₃₁NO₄
CAS No.:1312542-30-5
Molecular Formula:C₂₃H₃₁NO₄
Molecular Weight:385.503
Hs Code.:

C<sub>23</sub>H<sub>31</sub>NO<sub>4</sub>

Synonyms:C₂₃H₃₁NO₄

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Chemical Property of C₂₃H₃₁NO₄

Chemical Property:

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Technology Process of C₂₃H₃₁NO₄

There total 14 articles about C₂₃H₃₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1312542-29-2
C₂₅H₃₇NO₄Si

: 1312542-30-5
C₂₃H₃₁NO₄

Guidance literature:: With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate; In methanol; water; at 25 ℃; for 8h;
DOI:10.1021/ol201095b

Reference yield:

: 1199940-92-5
C₁₄H₂₄O₃Si

: 1312542-30-5
C₂₃H₃₁NO₄

Guidance literature:: Multi-step reaction with 13 steps

1.1: dichloromethane / 24 h / 25 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -30 °C / Inrtert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 25 °C

4.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

4.2: 0.5 h / -20 - 25 °C

5.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

6.1: pyridine / 6 h / 25 °C

7.1: 2 h / 180 °C / vacuum

8.1: tetrahydrofuran / 0.5 h / -30 °C

9.1: potassium hexamethylsilazane / diethylene glycol dimethyl ether; toluene / 1 h / 95 °C / Inert atmosphere

10.1: tetramethylammonium borohydride / tetrahydrofuran; water / 0.5 h / 0 °C

11.1: potassium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 25 °C

11.2: 1.5 h / 25 °C

12.1: tetrabutyl ammonium fluoride; water / tetrahydrofuran; N,N-dimethyl-formamide / 5 h / 65 °C

13.1: potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate / methanol; water / 8 h / 25 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium fluoride; samarium diiodide; tetrabutyl ammonium fluoride; water; dihydrogen peroxide; tetramethylammonium borohydride; potassium hydride; potassium hexamethylsilazane; diisobutylaluminium hydride; potassium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ol201095b

Reference yield:

: 1312542-05-4
C₃₀H₃₅NO₇SSi

: 1312542-30-5
C₂₃H₃₁NO₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -30 °C / Inrtert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 25 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

3.2: 0.5 h / -20 - 25 °C

4.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

5.1: pyridine / 6 h / 25 °C

6.1: 2 h / 180 °C / vacuum

7.1: tetrahydrofuran / 0.5 h / -30 °C

8.1: potassium hexamethylsilazane / diethylene glycol dimethyl ether; toluene / 1 h / 95 °C / Inert atmosphere

9.1: tetramethylammonium borohydride / tetrahydrofuran; water / 0.5 h / 0 °C

10.1: potassium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 25 °C

10.2: 1.5 h / 25 °C

11.1: tetrabutyl ammonium fluoride; water / tetrahydrofuran; N,N-dimethyl-formamide / 5 h / 65 °C

12.1: potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate / methanol; water / 8 h / 25 °C

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium fluoride; samarium diiodide; tetrabutyl ammonium fluoride; water; dihydrogen peroxide; tetramethylammonium borohydride; potassium hydride; potassium hexamethylsilazane; diisobutylaluminium hydride; potassium hydrogencarbonate; In tetrahydrofuran; methanol; dichloromethane; diethylene glycol dimethyl ether; water; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ol201095b