3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

Base Information

Chemical Name:3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether
CAS No.:1624284-62-3
Molecular Formula:C₂₇H₄₆OS
Molecular Weight:418.728
Hs Code.:

Synonyms:3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

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Chemical Property of 3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

Chemical Property:

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Technology Process of 3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

There total 6 articles about 3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1624284-58-7
(cis-4-(allyloxy)cyclohexyl)benzene

: 112-55-0
1-dodecylthiol

: 1624284-62-3
3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

: 1624284-65-6
2-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

Guidance literature:: With triethyl borane; 4-tert-Butylcatechol; In hexane; dichloromethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.201309984

Reference yield:

: 1624284-57-6
allyl trans-4-phenylcyclohexyl ether

: 112-55-0
1-dodecylthiol

: 1624284-60-1
3-dodecylsulfanylpropyl trans-4-phenylcyclohexyl ether

: 1624284-62-3
3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

: 1624284-63-4
2-dodecylsulfanylpropyl trans-4-phenylcyclohexyl ether

: 1624284-65-6
2-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In 1,4-dioxane; at 70 ℃; for 8h; Inert atmosphere;
DOI:10.1002/anie.201309984

Reference yield:

: 7335-12-8
cis-4-phenylcyclohexanol

: 1624284-62-3
3-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

: 1624284-65-6
2-dodecylsulfanylpropyl cis-4-phenylcyclohexyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / 0 - 40 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: triethyl borane; 4-tert-Butylcatechol / hexane; dichloromethane / 4 h / 20 °C / Inert atmosphere

With triethyl borane; 4-tert-Butylcatechol; sodium hydride; In hexane; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1002/anie.201309984