1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate

Base Information

Chemical Name:1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate
CAS No.:1392323-01-1
Molecular Formula:BF₄*C₁₅H₁₇F₆N₂
Molecular Weight:426.108
Hs Code.:

Synonyms:1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate

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Chemical Property of 1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate

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Technology Process of 1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate

There total 4 articles about 1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 13755-29-8
sodium tetrafluoroborate

: 1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium chloride

: 1392323-01-1
1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate

Guidance literature:: In acetonitrile; at 20 ℃; for 2h; Inert atmosphere; Sonication;
DOI:10.1021/acs.orglett.8b00321

Reference yield:

: 280-57-9,88935-43-7
1,4-diaza-bicyclo[2.2.2]octane

: 1392323-01-1
1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 18 h / 35 °C / Inert atmosphere

2: acetonitrile / 2 h / 20 °C / Inert atmosphere; Sonication

In diethyl ether; acetonitrile;
DOI:10.1021/acs.orglett.8b00321

Reference yield:

: 75462-59-8
3,5-bis(trifluoromethyl)benzyl chloride

: 1392323-01-1
1-(3,5-bis(trifluoromethyl)benzyl)-1,4-diazabicyclo[2.2.2]octan-1-ium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 18 h / 35 °C / Inert atmosphere

2: acetonitrile / 2 h / 20 °C / Inert atmosphere; Sonication

In diethyl ether; acetonitrile;
DOI:10.1021/acs.orglett.8b00321