tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate

Base Information

Chemical Name:tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate
CAS No.:1018690-27-1
Molecular Formula:C₂₁H₂₃F₂N₃O₃S
Molecular Weight:435.495
Hs Code.:

Synonyms:tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate

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Chemical Property of tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate

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Technology Process of tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate

There total 4 articles about tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 885060-36-6
2,5-difluoro-benzothiohydrazide

: 1018690-26-0
tert-butyl 3-oxo-3-phenyl-propoxycarbamate

: 1018690-27-1
tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate

Guidance literature:: In ethanol; at 20 ℃; for 16h;

Reference yield:

: 1018690-18-0
2-(2,5-difluoro-phenylcarbonothioylthio)acetic acid

: 1018690-27-1
tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; hydrazine / 14 h / 0 - 20 °C

2: ethanol / 16 h / 20 °C

With sodium hydroxide; hydrazine; In ethanol;

Reference yield:

: 1021853-64-4
C₇H₄F₂S₂

: 1018690-27-1
tert-butyl 2-(5-(2,5-difluorophenyl)-2-phenyl-2,3-dihydro-1,3,4-thiadiazol-2-yl)ethoxycarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water / 14 h / 20 °C

2: sodium hydroxide; hydrazine / 14 h / 0 - 20 °C

3: ethanol / 16 h / 20 °C

With sodium hydroxide; sodium hydrogencarbonate; hydrazine; In ethanol; water;