1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Base Information

Chemical Name:1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin
CAS No.:959918-99-1
Molecular Formula:C₈₄H₉₄N₆O₂₁
Molecular Weight:1523.7
Hs Code.:

Synonyms:1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

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Chemical Property of 1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

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Technology Process of 1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

There total 1 articles about 1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959919-00-7
4,6-di-O-acetyl-1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

: 959918-99-1
1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

Guidance literature:: 4",6"-di-O-acetyl-1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2"-di-O-benzyl-3,2',6',3"-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin; With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1.5h;

With sodium methylate; In methanol; chloroform; at 0 - 20 ℃; for 2h;

With acetic acid; In methanol; chloroform; at 0 ℃;

Reference yield: 41.0%

: 959918-99-1
1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2-di-O-benzyl-3,2',6',3-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin

: 1-N-[(S)-5-amino-2-hydroxypentanoyl]-2-hydroxydibekacin carbonate

Guidance literature:: 1-N-[(S)-5-amino-2-benzyloxy-N-benzyloxycarbonylpentanoyl]-2,2"-di-O-benzyl-3,2',6',3"-tetra-N-benzyloxycarbonyl-2-hydroxydibekacin; With hydrogenchloride; water; hydrogen; palladium; In 1,4-dioxane; at 20 ℃; for 14h;

With sodium hydrogencarbonate; In 1,4-dioxane; water;

With ammonia; water; hydrogen; acetic acid; palladium; more than 3 stages;