(S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester

Base Information

Chemical Name:(S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester
CAS No.:184223-10-7
Molecular Formula:C₂₈H₂₉N₃O₅S₂
Molecular Weight:551.687
Hs Code.:

Synonyms:(S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester

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Technology Process of (S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester

There total 1 articles about (S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-(Benzothiazole-2-sulfonylamino)-phenyl-acetic acid

: 184223-10-7
(S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / CH₂Cl₂ / Heating

2: 89 percent / aq. Na₂CO₃, aq. NaHCO₃ / CH₂Cl₂ / 0.25 h / 0 - 5 °C

With thionyl chloride; sodium hydrogencarbonate; sodium carbonate; In dichloromethane;
DOI:10.1021/ja961485n

Reference yield:

: 184223-10-7
(S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester

: 184223-25-4
(S)-2-((S)-2-Amino-2-phenyl-acetylamino)-3-phenyl-propionic acid tert-butyl ester

Guidance literature:: With hypophosphorous acid; In tetrahydrofuran; water; Heating;
DOI:10.1021/ja961485n

Reference yield:

: 184223-10-7
(S)-2-[(S)-2-(Benzothiazole-2-sulfonylamino)-2-phenyl-acetylamino]-3-phenyl-propionic acid tert-butyl ester

: (S)-2-((S)-2-Benzoylamino-2-phenyl-acetylamino)-3-phenyl-propionic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₃PO₂ / tetrahydrofuran; H₂O / Heating

2: NEt(i-Pr)2 / CH₂Cl₂

With hypophosphorous acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja961485n