N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine

Base Information

Chemical Name:N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine
CAS No.:1174376-32-9
Molecular Formula:C₁₂H₁₀F₂N₄O₂
Molecular Weight:280.234
Hs Code.:

Synonyms:N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine

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Chemical Property of N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine

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Technology Process of N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine

There total 3 articles about N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1174376-30-7
N'-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N,N dimethylformamidine

: 1174376-32-9
N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine

Guidance literature:: With hydroxylamine hydrochloride; In ethanol; at 50 ℃; for 1.5h;

Reference yield:

: 459-56-3
4-fluorobenzylic alcohol

: 1174376-32-9
N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / 1,4-dioxane / 0.17 h

1.2: 20 - 120 °C / Microwave irradiation

2.1: N,N-dimethyl-formamide / 16 h / 20 °C

3.1: hydroxylamine hydrochloride / ethanol / 1.5 h / 50 °C

With hydroxylamine hydrochloride; sodium hydride; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 1174376-11-4
5-fluoro-2-(4-fluorophenylmethoxy)pyrimidin-4 amine

: 1174376-32-9
N-[5-fluoro-2-(4-fluorobenzyloxy)pyrimidin-4-yl]-N'-hydroxyformamidine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 16 h / 20 °C

2: hydroxylamine hydrochloride / ethanol / 1.5 h / 50 °C

With hydroxylamine hydrochloride; In ethanol; N,N-dimethyl-formamide;