1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline

Base Information

Chemical Name:1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline
CAS No.:853792-78-6
Molecular Formula:C₂₀H₁₉N₃O
Molecular Weight:317.39
Hs Code.:

Synonyms:1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline

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Chemical Property of 1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline

Chemical Property:

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Technology Process of 1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline

There total 8 articles about 1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99009-85-5
N-(2-methylpropyl)-3-nitro-4-quinolinamine

: 853792-78-6
1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline

Guidance literature:: Multi-step reaction with 5 steps

1: H₂; MgSO₄ / Pt/C / ethyl acetate / 2740.88 Torr

2: dimethylformamide / 0.5 h / Heating

3: 10.4 g / NaOMe / methanol / 20 h / 20 °C

4: aq. KMnO₄ / acetic acid / 3 h / 20 °C

5: dimethylformamide / 1 h / Heating

With potassium permanganate; hydrogen; sodium methylate; magnesium sulfate; platinum on activated charcoal; In methanol; acetic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm049211v

Reference yield:

: 611-36-9
quinolin-4-ol

: 853792-78-6
1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline

Guidance literature:: Multi-step reaction with 8 steps

1: 81 percent / aq. HNO₃ / propionic acid / 0.25 h / 125 °C

2: SOCl₂; DMF / CH₂Cl₂ / 3 h / Heating

3: Et₃N / CH₂Cl₂ / 0.25 h / Heating

4: H₂; MgSO₄ / Pt/C / ethyl acetate / 2740.88 Torr

5: dimethylformamide / 0.5 h / Heating

6: 10.4 g / NaOMe / methanol / 20 h / 20 °C

7: aq. KMnO₄ / acetic acid / 3 h / 20 °C

8: dimethylformamide / 1 h / Heating

With potassium permanganate; thionyl chloride; hydrogen; nitric acid; sodium methylate; magnesium sulfate; triethylamine; N,N-dimethyl-formamide; platinum on activated charcoal; In methanol; dichloromethane; acetic acid; propionic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm049211v

Reference yield:

: 50332-66-6
3-nitro-quinolin-4-ol

: 853792-78-6
1-(2-methylpropyl)-2-phenoxy-1H-imidazo[4,5-c]quinoline

Guidance literature:: Multi-step reaction with 7 steps

1: SOCl₂; DMF / CH₂Cl₂ / 3 h / Heating

2: Et₃N / CH₂Cl₂ / 0.25 h / Heating

3: H₂; MgSO₄ / Pt/C / ethyl acetate / 2740.88 Torr

4: dimethylformamide / 0.5 h / Heating

5: 10.4 g / NaOMe / methanol / 20 h / 20 °C

6: aq. KMnO₄ / acetic acid / 3 h / 20 °C

7: dimethylformamide / 1 h / Heating

With potassium permanganate; thionyl chloride; hydrogen; sodium methylate; magnesium sulfate; triethylamine; N,N-dimethyl-formamide; platinum on activated charcoal; In methanol; dichloromethane; acetic acid; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm049211v