allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside

Base Information

Chemical Name:allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside
CAS No.:1179813-93-4
Molecular Formula:C₄₁H₄₇N₃O₁₉
Molecular Weight:885.833
Hs Code.:

Synonyms:allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside

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Technology Process of allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside

There total 2 articles about allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1179813-91-2
methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-D-galacto-nonulopyranosyl-N-phenyltrifluoroacetimidate

: 154391-03-4
allyl 2,3-di-O-benzoyl-α-D-galactopyranoside

: 1179813-93-4
allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; propiononitrile; at -78 ℃; optical yield given as %de; diastereoselective reaction; Microfluidic conditions;
DOI:10.1021/op900084f

Reference yield:

: 1179813-91-2
methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-D-galacto-nonulopyranosyl-N-phenyltrifluoroacetimidate

: 154391-03-4
allyl 2,3-di-O-benzoyl-α-D-galactopyranoside

: 1179813-93-4
allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-α-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside

: allyl 2,3-di-O-benzoyl-6-O-(methyl-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-azido-D-glycero-β-D-galacto-nonulopyranosyloate)-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In propiononitrile; at -78 ℃; for 4.5h; optical yield given as %de; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1002/asia.200800411