C₂₅H₂₄BP

Base Information

• Chemical Name: C₂₅H₂₄BP
• CAS No.: 1615699-48-3
• Molecular Formula: C₂₅H₂₄BP
• Molecular Weight: 366.25
• Mol file: 1615699-48-3.mol

Synonyms:C₂₅H₂₄BP

Chemical Property of C₂₅H₂₄BP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₄BP

There total 6 articles about C₂₅H₂₄BP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-biphenylboronic acid (5122-94-1) → C25H24BP (1615699-48-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenylphosphine; sodium carbonate / 1,2-dimethoxyethane; water / 85 °C

1.2: -78 °C

2.1: tetrahydrofuran / -78 °C

3.1: sulfuric acid

4.1: diethyl ether / -25 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sulfuric acid; sodium carbonate; triphenylphosphine; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; water; 1.1: |Suzuki-Miyaura Coupling;

DOI:10.1016/j.molcata.2014.04.026

Reference yield:

C18H13Li (1615699-80-3) → C25H24BP (1615699-48-3)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrahydrofuran / -78 °C

2: sulfuric acid

3: diethyl ether / -25 °C

With sulfuric acid; In tetrahydrofuran; diethyl ether;

DOI:10.1016/j.molcata.2014.04.026

Reference yield:

C25H24BOP (1615699-46-1) + methyllithium (917-54-4) → C25H24BP (1615699-48-3)

Guidance literature:

In diethyl ether; at -25 ℃;

DOI:10.1016/j.molcata.2014.04.026

upstream raw materials:

C₂₅H₂₄BOP

methyllithium

C₁₈H₁₃Li

4-biphenylboronic acid

Downstream raw materials:

C₂₅H₂₁P