methyl (3S,4S,5S)-3,4-diacetoxy-5-(tert-butyldimethylsilyloxy)-1-cyclohexenecarboxylate

Base Information

Chemical Name:methyl (3S,4S,5S)-3,4-diacetoxy-5-(tert-butyldimethylsilyloxy)-1-cyclohexenecarboxylate
CAS No.:1257516-70-3
Molecular Formula:C₁₈H₃₀O₇Si
Molecular Weight:386.518
Hs Code.:

Synonyms:methyl (3S,4S,5S)-3,4-diacetoxy-5-(tert-butyldimethylsilyloxy)-1-cyclohexenecarboxylate

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Chemical Property of methyl (3S,4S,5S)-3,4-diacetoxy-5-(tert-butyldimethylsilyloxy)-1-cyclohexenecarboxylate

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Technology Process of methyl (3S,4S,5S)-3,4-diacetoxy-5-(tert-butyldimethylsilyloxy)-1-cyclohexenecarboxylate

There total 1 articles about methyl (3S,4S,5S)-3,4-diacetoxy-5-(tert-butyldimethylsilyloxy)-1-cyclohexenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1257516-66-7
C₁₆H₂₈O₆Si

: 3396-11-0
cesium acetate

: 1257516-70-3
methyl (3S,4S,5S)-3,4-diacetoxy-5-(tert-butyldimethylsilyloxy)-1-cyclohexenecarboxylate

Guidance literature:: C₁₆H₂₈O₆Si; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.166667h; Inert atmosphere;

cesium acetate; With 18-crown-6 ether; In toluene; at 25 ℃; for 48h; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.molcatb.2010.07.009