3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide

Base Information

• Chemical Name: 3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide
• CAS No.: 946569-98-8
• Molecular Formula: C₃₁H₅₂N₄O₁₂
• Molecular Weight: 672.773

Synonyms:3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide

Chemical Property of 3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide

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Technology Process of 3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide

There total 1 articles about 3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

32-azido-3,6,9,12,15,18,21,24,27,30-decaoxadotriacontan-1-amine (912849-73-1) + 3-acetylbenzoic acid 2,5-dioxopyrrolidin-1-yl ester (946569-97-7) → 3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide (946569-98-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 72h;

Reference yield:

3-acetyl-N-[2-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2-azidoethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}-ethoxy)ethoxy]ethoxy}ethoxy)ethyl]benzamide (946569-98-8) + (S)-2-([Glu180,Asp182,Glu189]hGH(180-191)ylleucylamino)-3-(4-(prop-2-ynyloxy)phenyl)propionic amide (946569-96-6) → (S)-3-(4-((1-(2-(2-(2-(2-(2-(2-(2-(2-(2-(2-(2-(4-(acetyl)benzoylamino)ethoxy)ethoxy)ethoxy)-ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethyl)1,2,3-triazol-4-yl)methoxy)phenyl)-2-(([Glu180,Asp182,Glu189]hGH(180-191)yl)leucylamino)propionic amide (946569-99-9)

Guidance literature:

With 2,6-dimethylpyridine; copper(II) sulfate; ascorbic acid; In water; at 20 ℃; for 16h;

upstream raw materials:

32-azido-3,6,9,12,15,18,21,24,27,30-decaoxadotriacontan-1-amine

3-acetylbenzoic acid 2,5-dioxopyrrolidin-1-yl ester

Downstream raw materials:

(S)-3-(4-((1-(2-(2-(2-(2-(2-(2-(2-(2-(2-(2-(2-(4-(acetyl)benzoylamino)ethoxy)ethoxy)ethoxy)-ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethyl)1,2,3-triazol-4-yl)methoxy)phenyl)-2-(([Glu₁₈₀,Asp₁₈₂,Glu₁₈₉]hGH(180-191)yl)leucylamino)propionic amide

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