8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one

Base Information

Chemical Name:8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one
CAS No.:1350800-66-6
Molecular Formula:C₂₅H₁₅F₃N₂O₂
Molecular Weight:432.402
Hs Code.:

Synonyms:8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one

Chemical Property:

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Technology Process of 8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one

There total 5 articles about 8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₁₇F₃O₅

: 1350800-66-6
8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one

Guidance literature:: With hydrazine hydrate; acetic acid; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.09.042

Reference yield:

: 78326-88-2
5-benzyloxy-1-indanone

: 1350800-66-6
8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: selenium(IV) oxide / 1,4-dioxane / 3 h / Inert atmosphere; Reflux

2: acetic acid / 3 h / Inert atmosphere; Reflux

3: hydrazine hydrate; acetic acid / 20 °C / Inert atmosphere

With selenium(IV) oxide; hydrazine hydrate; acetic acid; In 1,4-dioxane;
DOI:10.1016/j.ejmech.2011.09.042

Reference yield:

: 3470-49-3
5-hydroxy-2,3-dihydro-1H-indene-1-one

: 1350800-66-6
8-(benzyloxy)-3-(3'-(trifluoromethyl)phenyl)-5H-indeno[1,2-c]pyridazin-5-one

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

2: selenium(IV) oxide / 1,4-dioxane / 3 h / Inert atmosphere; Reflux

3: acetic acid / 3 h / Inert atmosphere; Reflux

4: hydrazine hydrate; acetic acid / 20 °C / Inert atmosphere

With selenium(IV) oxide; potassium carbonate; hydrazine hydrate; acetic acid; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.09.042