C₃₆H₅₅N₅O₇S

Base Information

Chemical Name:C₃₆H₅₅N₅O₇S
CAS No.:1357008-03-7
Molecular Formula:C₃₆H₅₅N₅O₇S
Molecular Weight:701.928
Hs Code.:

C<sub>36</sub>H<sub>55</sub>N<sub>5</sub>O<sub>7</sub>S

Synonyms:C₃₆H₅₅N₅O₇S

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Chemical Property of C₃₆H₅₅N₅O₇S

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Technology Process of C₃₆H₅₅N₅O₇S

There total 13 articles about C₃₆H₅₅N₅O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₆H₅₇N₅O₇S

: 1357008-03-7
C₃₆H₅₅N₅O₇S

Guidance literature:: With pyridine; triethylamine; trifluoroacetic anhydride; In 1,2-dimethoxyethane; at 0 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 1357008-03-7
C₃₆H₅₅N₅O₇S

Guidance literature:: Multi-step reaction with 6 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: methoxybenzene; trifluoroacetic acid / dichloromethane

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

4: formic acid / 0.5 h / 60 °C

5: potassium hydrogencarbonate / 1,2-dimethoxyethane / 0.25 h / 20 °C / Inert atmosphere

6: pyridine; triethylamine; trifluoroacetic anhydride / 1,2-dimethoxyethane / 0 °C / Inert atmosphere

With pyridine; formic acid; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trifluoroacetic anhydride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/j.tet.2011.11.089

Reference yield:

: 114747-11-4
C₆H₁₄N₂S

: 1357008-03-7
C₃₆H₅₅N₅O₇S

Guidance literature:: Multi-step reaction with 3 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2: potassium hydrogencarbonate / 1,2-dimethoxyethane / 0.25 h / 20 °C / Inert atmosphere

3: pyridine; triethylamine; trifluoroacetic anhydride / 1,2-dimethoxyethane / 0 °C / Inert atmosphere

With pyridine; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic anhydride; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/j.tet.2011.11.089