5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Base Information

Chemical Name:5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione
CAS No.:87406-45-9
Molecular Formula:C₇₉H₈₂N₄O₁₁
Molecular Weight:1263.54
Hs Code.:

5,8-bis<2-<N-(t-butoxycarbonyl)-2-(trityloxy)ethylamino>ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Synonyms:5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

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Chemical Property of 5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

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Technology Process of 5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

There total 6 articles about 5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 77-78-1
dimethyl sulfate

: 87406-44-8
5,8-bis<2-ethylamino>-1-hydroxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

: 87406-45-9
5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Guidance literature:: With potassium carbonate; In acetone; for 6h; Heating;
DOI:10.1246/bcsj.56.1812

Reference yield:

: 76-83-5
trityl chloride

: 87406-45-9
5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine / 17 h / 60 °C

2: 87 percent / K₂CO₃ / dimethylformamide; CH₂Cl₂ / 4 h

3: 77 percent / K₂CO₃ / acetone / 6 h / Heating

With pyridine; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1246/bcsj.56.1812

Reference yield:

: 87406-40-4
2-(t-butoxycarbonyloxy)-5,8-bis<2-(N-t-butoxycarbonyl-2-hydroxyethylamino)ethylamino>-1-hydroxy-9,10-anthracenedione

: 87406-45-9
5,8-bis<2-ethylamino>-1-methoxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / pyridine / 17 h / 60 °C

2: 94 percent / K₂CO₃ / acetone / 7 h / Heating

3: 87 percent / K₂CO₃ / dimethylformamide; CH₂Cl₂ / 4 h

4: 77 percent / K₂CO₃ / acetone / 6 h / Heating

With pyridine; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1246/bcsj.56.1812