C₃₆H₅₇ClO₄SSi₂

Base Information

Chemical Name:C₃₆H₅₇ClO₄SSi₂
CAS No.:1547297-52-8
Molecular Formula:C₃₆H₅₇ClO₄SSi₂
Molecular Weight:677.536
Hs Code.:

C<sub>36</sub>H<sub>57</sub>ClO<sub>4</sub>SSi<sub>2</sub>

Synonyms:C₃₆H₅₇ClO₄SSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₆H₅₇ClO₄SSi₂

Chemical Property:

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Technology Process of C₃₆H₅₇ClO₄SSi₂

There total 6 articles about C₃₆H₅₇ClO₄SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 842132-50-7
1,5-anhydro-2-deoxy-4,6-O-di-(tert-butyl)silanediyl-3-O-triisopropylsilyl-D-arabino-hex-1-enitolylboronic acid pinacol ester

: 1057216-05-3
5-bromo-2-chloro-3-(4-ethylbenzyl)thiophene

: 1547297-52-8
C₃₆H₅₇ClO₄SSi₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In 1,2-dimethoxyethane; water; for 4h; Reflux;
DOI:10.1248/cpb.c13-00407

Reference yield:

: 120759-16-2
5-bromo-2-chlorothiophene-3-carbaldehyde

: 1547297-52-8
C₃₆H₅₇ClO₄SSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0.5 h / 0 °C

2: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 1 h / -78 - 20 °C

3: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; water / 4 h / Reflux

With triethylsilane; bis-triphenylphosphine-palladium(II) chloride; boron trifluoride diethyl etherate; sodium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1248/cpb.c13-00407

Reference yield:

: 1547297-60-8
(5-bromo-2-chloro-3-thienyl)(4-ethylphenyl)methanol

: 1547297-52-8
C₃₆H₅₇ClO₄SSi₂

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate; triethylsilane / dichloromethane / 1 h / -78 - 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; water / 4 h / Reflux

With triethylsilane; bis-triphenylphosphine-palladium(II) chloride; boron trifluoride diethyl etherate; sodium carbonate; In 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1248/cpb.c13-00407