(R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine

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Chemical Name:(R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine
CAS No.:160256-03-1
Molecular Formula:C₃₁H₃₃NO₆S
Molecular Weight:547.672
Hs Code.:

Synonyms:(R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine

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Chemical Property of (R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine

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Technology Process of (R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine

There total 7 articles about (R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 160256-02-0
(+)-(R)-2-(2'-methoxynaphthyl-1'-sulfinyl)-3,4-dimethoxyacetophenone

: 160256-03-1
(R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 20h; Heating; azeotropic sepn. of water;
DOI:10.1016/S0040-4020(01)89357-1

Reference yield: 65.0%

: 155135-07-2
(-)-(1R,2S,5R)-menthyl (S)-2-methoxynaphthalene-1-sulfinate

: [2-(3,4-Dimethoxy-phenyl)-ethyl]-[1-(3,4-dimethoxy-phenyl)-eth-(E)-ylidene]-amine

: 160256-03-1
(R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/S0040-4020(01)89357-1

Reference yield:

: 155135-07-2
(-)-(1R,2S,5R)-menthyl (S)-2-methoxynaphthalene-1-sulfinate

: 160256-03-1
(R)-N-<2-(2'-methoxy-1'-naphthylsulfinyl)-1-(3',4'-dimethoxyphenyl)>ethenyl-N-<2-(3'-4'-dimethoxyphenyl)>ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / benzene; diethyl ether / 2 h / Ambient temperature

2: 50 percent / lithium diisopropylamide / tetrahydrofuran / 1.) -78 deg C, 30 min; 2. r.t.

3: 86 percent / p-toluenesulfonic acid / benzene / 20 h / Heating; azeotropic sepn. of water

With toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)89357-1